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可靠性灵敏度 3

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Effect of potassium carbonate on catalytic synthesis of calcium carbide at moderate temperature

Dejun SHI, Ke QIAO, Zifeng YAN

《化学科学与工程前沿（英文）》 2011年 第5卷 第3期   页码 372-375 doi: 10.1007/s11705-010-0570-1

摘要： Calcium carbide was successfully synthesized by carbothermal reduction of lime with coke at 1973 K for 1.5 h. The effect of potassium carbonate as additive on the composition and morphology of the product was investigated using X-ray diffraction and scanning electron microscope. Addition of potassium carbonate increased the yield of calcium carbide. The sample in the presence of potassium carbonate generated acetylene gas of 168.3 L/kg, which was 10% higher than that in the absence of potassium carbonate. This result confirmed the catalytic effect of potassium carbonate on the synthesis of calcium carbide. A possible mechanism of the above effects was that the additive, which was melted at the reduction temperature, dissolved CaO and so promoted the contact between CaO and carbon, which was essential for the solid-solid reaction to form calcium carbide.

关键词： calcium carbide     synthesis     catalysis    

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Influences of additives on the crystal habit of potassium chloride

Xiaofu GUO, Junsheng YUAN, Zhiyong JI, Min SU,

《化学科学与工程前沿（英文）》 2010年 第4卷 第1期   页码 78-81 doi: 10.1007/s11705-009-0300-8

摘要： By means of constant control speed cooling crystallization, the influences of four additives, including lead chloride, cadmium chloride, sodium salicylate, and quaternary ammonium salt, on the crystal habit of KCl were investigated. The results show that the crystal habit of KCl is cube without additives, the crystal habit of KCl is ellipsoid-like in the presence of Pb, the crystal habit of KCl is strip in the presence of Cd, and the crystal habit of KCl is cavate cube in the presence of sodium salicylate. X-ray diffractometry analysis reveals that these additives can change the crystal habit of KCl but not its crystal structure.

关键词： cadmium chloride     salicylate     presence     crystallization     diffractometry analysis    

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Experimental study on high-efficiency polishing for potassium dihydrogen phosphate (KDP) crystal by using

Ziyuan LIU, Hang GAO, Dongming GUO

《机械工程前沿（英文）》 2020年 第15卷 第2期   页码 294-302 doi: 10.1007/s11465-019-0576-4

摘要： A high-efficiency polishing approach using two-phase air–water fluid (TAWF) is proposed to avoid surface contamination and solve the inefficiency of previous water-dissolution polishing techniques for potassium dihydrogen phosphate (KDP) crystal. In the proposed method, controllable deliquescence is implemented without any chemical impurity. The product of deliquescence is then removed by a polishing pad to achieve surface planarization. The mechanism underlying TAWF polishing is analyzed, a special device is built to polish the KDP crystal, and the effect of relative humidity (RH) on polishing performance is studied. The relationship between key parameters of polishing and surface planarization is also investigated. Results show that the polishing performance is improved with increasing RH. However, precisely controlling the RH is extremely difficult during TAWF polishing. Controllable deliquescence can easily be disrupted once the RH fluctuates, which therefore needs to be restricted to a low level to avoid its influence on deliquescence rate. The material removal of TAWF polishing is mainly attributed to the synergistic effect of deliquescence and the polishing pad. Excessive polishing pressure and revolution rate remarkably reduce the life of the polishing pad and the surface quality of the KDP crystal. TAWF polishing using IC-1000 and TEC-168S increase the machining efficiency by 150%, and a smooth surface with a root mean square surface roughness of 5.5 nm is obtained.

关键词： potassium dihydrogen phosphate (KDP) crystal     controllable deliquescence     two-phase air–water fluid     high-efficiency polishing     material removal    

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A space power system of free piston Stirling generator based on potassium heat pipe

Mingqiang LIN, Jian MOU, Chunyun CHI, Guotong HONG, Panhe GE, Gu HU

《能源前沿（英文）》 2020年 第14卷 第1期   页码 1-10 doi: 10.1007/s11708-019-0655-6

摘要： The power system of a free piston Stirling generator (FPSG) based on potassium heat pipes has been developed in this paper. Thanks to the advantages of long life, high reliability, and high overall thermal efficiency, the FPSG is a promising candidate for nuclear energy, especially in space exploration. In this paper, the recent progress of FPSG based on nuclear reactor for space use was briefly reviewed. A novel FPSG weighted only 4.2 kg was designed, and one dimensional thermodynamic modeling of the FPSG using Sage software was performed to estimate its performance. The experiment results indicated that this FPSG could provide 142.4 W at a thermal-to-electric efficiency of nearly 17.4%. Besides, the power system integrated with four FPSGs and potassium heat pipes was performed and the single machine failure test was conducted. The results show that this system could provide an electrical power of 300 W at an overall thermal efficiency of 7.3%. Thus, it is concluded that this power system is feasible and will have a great prospect for future applications.

关键词： free piston Stirling generator (FPSG)     potassium heat pipe     power system     energy conversion    

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Effect of adding a smart potassium ion-responsive copolymer into polysulfone support membrane on the

Meibo He, Zhuang Liu, Tong Li, Chen Chen, Baicang Liu, John C. Crittenden

《化学科学与工程前沿（英文）》 2019年 第13卷 第2期   页码 400-414 doi: 10.1007/s11705-018-1757-0

摘要： Thin-film composite (TFC) nanofiltration (NF) membranes were fabricated via the interfacial polymerization of piperazine (PIP) and 1,3,5-benzenetricarbonyl trichloride on polysulfone (PSf) support membranes blended with K -responsive poly( -isopropylacryamide-co-acryloylamidobenzo-15-crown-5) (P(NIPAM-co-AAB C )). Membranes were characterized by attenuated total reflection Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, atomic force microscope, scanning electron microscope, contact angle, and filtration tests. The results showed that: (1) Under K -free conditions, the blended P(NIPAM-co-AAB C )/PSf supports had porous and hydrophilic surfaces, thereby producing NF membranes with smooth surfaces and low MgSO rejections; (2) With K in the PIP solution, the surface roughness and water permeability of the resultant NF membrane were increased due to the K -induced transition of low-content P(NIPAM-co-AAB C ) from hydrophilic to hydrophobic; (3) After a curing treatment at 95 °C, the improved NF membrane achieved an even higher pure water permeability of 10.97 L·m ·h ·bar under 200 psi. Overall, this study provides a novel method to improve the performance of NF membranes and helps understand the influence of supports on TFC membranes.

关键词： nanofiltration     interfacial polymerization     support membrane     potassium ion-responsive     thin-film composite    

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Research on acoustic-structure sensitivity using FEM and BEM

ZHANG Jun, ZHAO Wenzhong, ZHANG Weiying

《机械工程前沿（英文）》 2007年 第2卷 第1期   页码 62-67 doi: 10.1007/s11465-007-0010-1

摘要： Acoustic-structure sensitivity is used to predict the change of acoustic pressure when a structure design variable is changed. The sensitivity is significant for reducing noise of structure. Using FEM (finite element method) and BEM (boundary element method) acoustic-structure sensitivity was formulated and presented. The dynamic response and response velocity sensitivity with respect to structure design variable were carried out by using structural FEM, the acoustic response and acoustic pressure sensitivity with respect to structure velocity were carried out by using acoustic BEM. Then, acoustic-structure sensitivity was computed by linking velocity sensitivity in FEM and acoustic sensitivity in BEM. This method was applied to an empty box as an example. Acoustic pressure sensitivity with respect to structure thickness achieved in frequency ranges 1 100 Hz, and its change rule along with stimulating frequency and design variable were analyzed. Results show that acoustic-structure sensitivity method linked with FEM and BEM is effective and correct.

关键词： sensitivity method     BEM     acoustic pressure     pressure sensitivity     frequency    

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Parametric sensitivity analysis of cellular diaphragm wall

Xi CHEN, Wei XU

《结构与土木工程前沿（英文）》 2012年 第6卷 第4期   页码 358-364 doi: 10.1007/s11709-012-0177-3

摘要： The deformation law of the cellular diaphragm wall in deep foundation pits was studied through numerical simulation. Based on the example of the dock wall in engineering, the full three-dimensional finite element model was used to simulate the excavation of the foundation pit. Interaction between the cellular diaphragm wall and the soil was also taken into account in the calculation. The results indicated that the maximum lateral displacement, which is the evaluation index of sensitivity analysis, appeared on the top of the interior longitudinal wall with an excavation depth of 10 m. The centrifuge model test was carried out to study the deformation regulation for a cellular diaphragm wall. The most sensitive factor was found by adjusting the length of the partition wall, the spacing of the partition wall and the thickness of the wall. In the end, a suggestion was proposed to optimize the cellular diaphragm by adjusting the length of the partition wall.

关键词： cellular diaphragm wall     sensitivity analysis     optimization     centrifuge model test    

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Probability strength design of steam turbine blade and sensitivity analysis with respect to random parameters

DUAN Wei

《能源前沿（英文）》 2008年 第2卷 第1期   页码 107-115 doi: 10.1007/s11708-008-0018-1

摘要： Many stochastic parameters have an effect on the reliability of a steam turbine blade during practical operation. To improve the reliability of blade design, it is necessary to take these stochastic parameters into account. An equal cross-section blade is investigated and a finite element model is built parametrically. Geometrical parameters, material parameters and load parameters of the blade are considered as input random variables while the maximum deflection and maximum equivalent stress are output random variables. Analysis file of the blade is compiled by deterministic finite element method and applied to be loop file to create sample points. A quadratic polynomial with cross terms is chosen to regress these samples by step-forward regression method and employed as a surrogate of numerical solver to drastically reduce the number of solvers call. Then, Monte Carlo method is used to obtain the statistical characteristics and cumulative distribution function of the maximum deflection and maximum equivalent stress of the blade. Probability sensitivity analysis, which combines the slope of the gradient and the width of the scatter range of the random input variables, is applied to evaluate how much the output parameters are influenced by the random input parameters. The scatter plots of structural responses with respect to the random input variables are illustrated to analyze how to change the input random variables to improve the reliability of the blade. The results show that combination of the finite element method, the response surface method and Monte Carlo method is an ideal way for the reliability analysis and probability strength design of the blade.

关键词： Probability sensitivity     sensitivity analysis     number     cross-section     statistical    

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Preparation and gaseous photocatalytic activity of smooth potassium dititanate film

QIAN Qinghua, HU Yuyan, WEN Gaofei, FENG Xin, LU Xiao-hua

《化学科学与工程前沿（英文）》 2008年 第2卷 第3期   页码 308-314 doi: 10.1007/s11705-008-0047-7

摘要： A new smooth potassium dititanate film was prepared by sol-gel method and characterized by thermogravimetry (TG) and differential scanning calorimetry (DSC), X-ray diffraction (XRD), atomic force microscopy (AFM), UV-Visible diffuse reflectance and Raman spectroscopy. The gaseous photocatalytic activity of smooth KTiO films was studied using contact angle analysis from the photocatalytic decomposition of octadecyltrichlorosilane (OTS) based self-assembled monolayers (SAMs) formed on KTiO films. The photocurrent response of the film was determined by an electrochemical method. It was shown that the films were smooth, compact, and transparent when formed on glass. Compared with TiO film, the KTiO film showed wide absorption in the ultraviolet and visible region. It was found that the monolayers on KTiO decomposed much faster than those on TiO under UV irradiation of 254 nm in air. The film also exhibited a stronger photoresponse and a more stable anodic photocurrent. The KTiO film efficiently decomposes the alkylsiloxane monolayers under UV irradiation in air and it was found to be a good photocatalyst for gaseous organic pollutant treatment.

关键词： reflectance     UV-Visible     photocurrent     irradiation     scanning calorimetry    

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Genetic variants in the ADD1 and GNB3 genes and blood pressure response to potassium supplementation

Dai-Hai YU PhD, Jian-Feng HUANG MD, Ji-Chun CHEN MS, Jie CAO MS, Shu-Feng CHEN PhD, Dong-Feng GU MD, PhD, for the GenSalt Collaborative Research Group, De-Pei LIU PhD, Lai-Yuan WANG PhD, Jing CHEN MD, MSc, Jiang HE MD, PhD, Cashell E. JAQUISH PhD, Dabeeru C. RAO PhD, Charles GU PhD, James E. HIXSON PhD, Chung-Shiuan CHEN MS8, Paul K. WHELTON MD, MSc9,

《医学前沿（英文）》 2010年 第4卷 第1期   页码 59-66 doi: 10.1007/s11684-010-0015-8

摘要： Dietary potassium-supplementation has been associated with a decreased risk of hypertension and other cardiovascular outcomes. However, blood pressure (BP) responses to potassium supplementation vary among individuals. This study was designed to examine the association between 12 single nucleotide polymorphisms (SNPs) in the adducin 1 alpha (ADD1) and guanine nucleotide binding protein (G protein) beta polypeptide 3 (GNB3) genes and systolic BP (SBP), diastolic BP (DBP), and mean arterial pressure (MAP) responses to potassium-supplementation. We conducted a 7-day high-sodium intervention (307.8 mmol sodium/day) followed by a 7-day high-sodium with potassium-supplementation (60 mmol potassium/day) among 1906 Han Chinese participants from rural north China. BP measurements were obtained at the end of each intervention period using a random-zero sphygmomanometer. We identified significant associations between ADD1 variant rs17833172 and SBP, DBP, and MAP responses to potassium-supplementation (all <0.0001) that remained significant after adjustment for multiple comparisons. In participants that were heterozygous or homozygous for the G allele of this marker, SBP, DBP, and MAP response to potassium-supplementation were −3.52 (−3.82, −3.21), −1.41 (−1.66, −1.15) and −2.12 (−2.37, −1.87), respectively, as compared to the corresponding responses of 1.99 (0.25, 3.73), −0.65 (−0.10, −0.21), and −0.23 (−0.37, 0.83), respectively, for those who were homozygous for A allele. In addition, participants with at least one copy of the G allele of rs12503220 of the ADD1 gene had significantly increased DBP and MAP response to potassium-supplementation ( = 0.0041 and 0.01, respectively), which was also significant after correction for multiple testing. DBP and MAP responses to potassium-supplementation were −1.36 (−1.63, −1.10) and −2.07 (−2.32, −1.82) for those with at least G allele compared to corresponding responses of 0.86 (−0.68, 2.40) and −0.45 (−1.74, 0.84) for those who were homozygous for A allele. In summary, our study identified novel associations between genetic variants of the ADD1 gene and BP response to potassium-supplementation, which could have important clinical and public health implications. Future studies aimed at replicating these novel findings are warranted.

关键词： blood pressure     genetics     polymorphism     die-tary potassium     potassium sensitivity     adducin 1 alpha (ADD1)     guanine nucleotide binding protein beta polypeptide 3 (GNB3)    

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Wheel tracking methods to evaluate moisture sensitivity of hot-mix asphalt mixtures

Jie HAN,Harihar Shiwakoti

《结构与土木工程前沿（英文）》 2016年 第10卷 第1期   页码 30-43 doi: 10.1007/s11709-016-0318-1

摘要： Existing test methods to determine moisture sensitivity in hot-mix asphalt (HMA) mixtures are time consuming and inconsistent. This research focused on wheel tracking devices to evaluate moisture sensitivity. The Asphalt Pavement Analyzer (APA) and the Hamburg Wheel Tracking Device (HWTD) were used for this research. Compacted cylindrical samples were fabricated using a Superpave Gyratory compactor. This study selected two most commonly used mixtures, SM-12.5A with PG 64-22 binder in overlay projects and SM-19A mixtures with PG 64-22 binder for major modification projects at Kansas Department of Transportation. Test results show that APA tests could induce stripping in most samples without any anti-stripping agent, which could be identified visually. However, APA results did not indicate any stripping inflection point while the HWTD results showed stripping inflection points, which are important to identify stripping potential of mixtures. The APA results show that wet tests are severe at lower temperatures. The HWTD results show improvement in the performance using anti-stripping agents at later stage. The HWTD test is more effective as a rapid test method in case of determining moisture sensitivity. Laboratory results from this study should be verified and correlated with field performance.

关键词： hot-mix asphalt     moisture sensitivity     rutting     wheel tracking test    

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Catalytic process modeling and sensitivity analysis of alkylation of benzene with ethanol over MIL-101

Ehsan Rahmani, Mohammad Rahmani

《化学科学与工程前沿（英文）》 2020年 第14卷 第6期   页码 1100-1111 doi: 10.1007/s11705-019-1891-3

摘要： A solvothermal method was used to synthesize MIL-101(Fe) and MIL-88(Fe), which were used for alkylation of benzene. The synthesized catalysts were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, field emission scanning electron microscope, dynamic light scattering, and BET techniques. Metal-organic frameworks (MOFs) were modeled to investigate the catalytic performance and existence of mass transfer limitations. Calculated effectiveness factors revealed absence of internal and external mass transfer. Sensitivity analysis revealed best operating conditions over MIL-101 at 120°C and 5 bar and over MIL-88 at 142°C and 9 bar.

关键词： MOFs     alkylation     ethylbenzene     catalysts pellet model     kinetic model     sensitivity analysis    

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An antibiotic composite electrode for improving the sensitivity of electrochemically active biofilm biosensor

《环境科学与工程前沿（英文）》 2022年 第16卷 第8期 doi: 10.1007/s11783-022-1518-7

摘要：

• Antibiotic azithromycin employed in graphite electrode for EAB biosensor.

关键词： AZM@GP composite electrode     EAB-biosensor     Water quality early-warning    

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Global sensitivity analysis of certain and uncertain factors for a circular tunnel under seismic action

Nazim Abdul NARIMAN, Raja Rizwan HUSSAIN, Ilham Ibrahim MOHAMMAD, Peyman KARAMPOUR

《结构与土木工程前沿（英文）》 2019年 第13卷 第6期   页码 1289-1300 doi: 10.1007/s11709-019-0548-0

摘要： There are many certain and uncertain design factors which have unrevealed rational effects on the generation of tensile damage and the stability of the circular tunnels during seismic actions. In this research paper, we have dedicated three certain and four uncertain design factors to quantify their rational effects using numerical simulations and the Sobol’s sensitivity indices. Main effects and interaction effects between the design factors have been determined supporting on variance-based global sensitivity analysis. The results detected that the concrete modulus of elasticity for the tunnel lining has the greatest effect on the tensile damage generation in the tunnel lining during the seismic action. In the other direction, the interactions between the concrete density and both of concrete modulus of elasticity and tunnel diameter have appreciable effects on the tensile damage. Furthermore, the tunnel diameter has the deciding effect on the stability of the tunnel structure. While the interaction between the tunnel diameter and concrete density has appreciable effect on the stability process. It is worthy to mention that Sobol’s sensitivity indices manifested strong efficiency in detecting the roles of each design factor in cooperation with the numerical simulations explaining the responses of the circular tunnel during seismic actions.

关键词： shear waves     Sobol’s sensitivity indices     maximum principal stress     maximum overall displacement     tensile damage    

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Kinetics of oxidation of dimethyl trisulfide by potassium permanganate in drinking water

Xiaoyan MA, Shifei HU, Hongyu WANG, Jun LI, Jing HUANG, Yun ZHANG, Weigang LU, Qingsong LI

《环境科学与工程前沿（英文）》 2012年 第6卷 第2期   页码 171-176 doi: 10.1007/s11783-011-0319-1

摘要： Metabolites of algae such as geosmin, 2-methylisoborneol etc. are reported to induce pungent odors into drinking water and attract additional scientific attention. Recently, in China, taste and odor outbreaks in drinking water supply have become increasingly common. In source water affected by eutrophication, dimethyl trisulfide, speculated to be produced by decayed algae, was found to be the source of taste and odor issues and can be removed effectively by usual oxidation agents. In this experimental study, batch scale tests were carried out focusing on the removal of dimethyl trisulfide. Reaction kinetics of dimethyl trisulfide oxidized by potassium permanganate in water had been studied; influence factors such as pH, organic substrate, other existed taste, and odor contaminant in equivalent concentration were also discussed. Results showed that dimethyl trisulfide can be removed by potassium permanganate efficiently; the ratio can reach more than 70% with oxidant dosage of 4 mg·L and contact time prolonged to 120 min. The dimethyl trisulfide decomposition followed a second-order kinetics pattern with a rate constant = 0.00213 L·(min·mg) . Typically, the degradation rate of dimethyl trisulfide was increased with the increasing KMnO dosage, but dramatically dropped with the increasing levels of humic acid (1.8–4.5 mg·L ) and other odor-causing compounds (e.g. -cyclocitral, 0–1886.0 μg·L ). Solution pH (5.2–9.0) and initial dimethyl trisulfide concentration did not significantly affected the degradation. This study demonstrates that KMnO oxidation is an effective option to remove dimethyl trisulfide from water.

关键词： odor and taste     oxidation reaction     reaction kinetics     water treatment    

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标题 作者 时间 类型 操作

Effect of potassium carbonate on catalytic synthesis of calcium carbide at moderate temperature

Dejun SHI, Ke QIAO, Zifeng YAN

期刊论文

Influences of additives on the crystal habit of potassium chloride

Xiaofu GUO, Junsheng YUAN, Zhiyong JI, Min SU,

期刊论文

Experimental study on high-efficiency polishing for potassium dihydrogen phosphate (KDP) crystal by using

Ziyuan LIU, Hang GAO, Dongming GUO

期刊论文

A space power system of free piston Stirling generator based on potassium heat pipe

Mingqiang LIN, Jian MOU, Chunyun CHI, Guotong HONG, Panhe GE, Gu HU

期刊论文

Effect of adding a smart potassium ion-responsive copolymer into polysulfone support membrane on the

Meibo He, Zhuang Liu, Tong Li, Chen Chen, Baicang Liu, John C. Crittenden

期刊论文

Research on acoustic-structure sensitivity using FEM and BEM

ZHANG Jun, ZHAO Wenzhong, ZHANG Weiying

期刊论文

Parametric sensitivity analysis of cellular diaphragm wall

Xi CHEN, Wei XU

期刊论文

Probability strength design of steam turbine blade and sensitivity analysis with respect to random parameters

DUAN Wei

期刊论文

Preparation and gaseous photocatalytic activity of smooth potassium dititanate film

QIAN Qinghua, HU Yuyan, WEN Gaofei, FENG Xin, LU Xiao-hua

期刊论文

Genetic variants in the ADD1 and GNB3 genes and blood pressure response to potassium supplementation

Dai-Hai YU PhD, Jian-Feng HUANG MD, Ji-Chun CHEN MS, Jie CAO MS, Shu-Feng CHEN PhD, Dong-Feng GU MD, PhD, for the GenSalt Collaborative Research Group, De-Pei LIU PhD, Lai-Yuan WANG PhD, Jing CHEN MD, MSc, Jiang HE MD, PhD, Cashell E. JAQUISH PhD, Dabeeru C. RAO PhD, Charles GU PhD, James E. HIXSON PhD, Chung-Shiuan CHEN MS8, Paul K. WHELTON MD, MSc9,

期刊论文

Wheel tracking methods to evaluate moisture sensitivity of hot-mix asphalt mixtures

Jie HAN,Harihar Shiwakoti

期刊论文

Catalytic process modeling and sensitivity analysis of alkylation of benzene with ethanol over MIL-101

Ehsan Rahmani, Mohammad Rahmani

期刊论文

An antibiotic composite electrode for improving the sensitivity of electrochemically active biofilm biosensor

期刊论文

Global sensitivity analysis of certain and uncertain factors for a circular tunnel under seismic action

Nazim Abdul NARIMAN, Raja Rizwan HUSSAIN, Ilham Ibrahim MOHAMMAD, Peyman KARAMPOUR

期刊论文

Kinetics of oxidation of dimethyl trisulfide by potassium permanganate in drinking water

Xiaoyan MA, Shifei HU, Hongyu WANG, Jun LI, Jing HUANG, Yun ZHANG, Weigang LU, Qingsong LI

期刊论文